Collection paper in museums and libraries and stores suffer from acid hydrolysis and oxidations, many factors catalysis the deterioration by acid hydrolysis and oxidations, such as humidity and temperature and light and fungi, paper contains iron ink and colors based on ions heavy metals such as copper and zinc, air pollution, visible and industry light, Residues of manufacturing processes such as bleaching material, additives such as sizing materials, The study proposes a new antioxidants agent by using Line seed gel with magnesium bicarbonate loaded with Zinc oxide (NP), the positive impact of this treatment was evaluated on thermally accelerated ageing on cotton, linen and wooden samples, the samples was verified by FTIR, tensile strength and elongation measurement, Measurement of color change, PH measurement, aromatic hydroxylation assay, (SEM) scanning Electron microscope, Linseed gel with MgHCO3 and Zinc oxide (NP) results to stabilize inks and stop oxidation that occurred and treatment of free radicals, the inks were most stable, The mechanical properties of the samples have been greatly improved, Linseed gel with magnesium bicarbonate loaded with Zinc oxide (NP) consolidation and treatment the samples, the zinc oxide (NP) nano oxide was observed between the fibers which works to protect the cellulose fibers From degradation.
Published in | International Journal of Archaeology (Volume 8, Issue 1) |
DOI | 10.11648/j.ija.20200801.12 |
Page(s) | 6-14 |
Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
Copyright |
Copyright © The Author(s), 2020. Published by Science Publishing Group |
Carbonyl Groups, Ageing, Potassium Permanganate, C=O Vibration
[1] | Rouchon, V., Duranton, M., Burgaud, C., Pellizzi, E., Lavedrine, B., Janssens, K., de Nolf, W., Nuyts, G., Vanmeert, F., & Hellemans, K. (2011) Room-temperature study of iron gall ink impregnated paper degradation under various oxygen and humidity conditions: Time-dependent monitoring by viscosity and X-ray absorption near-edge spectrometry measurements. Analytical Chemistry, 83, 2589–2597. DOI: 10.1021/ac1029242. |
[2] | Ferrer, N., M, C, Sistach. (2007) FTIR technique used to study acidic paper manuscripts dating from the thirteen to sixteen century from the archive of crown of Argon. B. paper, Gr, Annu 26: 21-25. I. S. Jacobs and C. P. Bean, “Fine particles, thin films and exchange anisotropy,” in Magnetism, vol. III, G. T. Rado and H. Suhl, Eds. New York: Academic, 1963, pp. 271–350. |
[3] | Zervos, S. (2010) Natural and accelerated ageing of cellulose and paper: A literature review. In A. Lejeune & T. Deprez (Eds.), Cellulose: Structure and Properties, Derivatives and Industrial Uses. New York: Nova Publishing. |
[4] | Yasin Zidan, Ahmed ElShafei, Wafika Noshy and Eman Salim. (2017) A comparative study to evaluate conventional and nonconventional cleaning treatments of cellulosic paper supports. Mediterranean Archaeology and Archaeometry, Vol. 17, No 3, pp. 337-353. DOI: 10.5281/zenodo.1005538. |
[5] | Pedersoli Junior, JL, Reisland B., Risk. (2003) Assessment: A tool to compare alternative courses of action for the conservation of iron-gall ink containing objects. Restaur 24: 205-226. |
[6] | Wahba, Wafika Noshy., Fahmi, Abdelgawad Ali., Nagaty, Eman Shalaby. (2019) the evaluation of the efficacy of two magnesium based deacidification methods on the stability of three different types of papers, International Journal of Conservation Science. Apr-Jun 2019, Vol. 10 Issue 2, p235-248. 14p. |
[7] | Malešič, J., Kolar, J., Anders, M. (2015) Evaluation of Treatments for Stabilization of Verdigris and Malachite Containing Paper Document. Article in Restaurator 36 (4): 283-305. |
[8] | Neevel, JG., (1995) Phytate: a potential conservation agent for the treatment of lnk corrosion caused by iron gall inks. Restaur 16: 143-160. |
[9] | Panayotova, T., Dimova Todorova, M., Dobrevsky, I. (2007) Purification and reuse of heavy metals contain-ing wastewaters from electroplating plants. Desalin. 206, 135-140. |
[10] | Malešič, J., Kočar, D., Balazic, A. (2012) Stabilization of copper and iron containing papers in mildly alkaline environment. Polymer Degrad Stab. 97, 118-123. |
[11] | Singh, K., Mridual, D., Rehal, J. (2011) Flaxseed: a potential source of food, feel and fiber. Crit. rev. food sci, 51 (3): 210-22, doi: 10.1080/10408390903537241. J. Clerk Maxwell, A Treatise on Electricity and Magnetism, 3rd ed., vol. 2. Oxford: Clarendon, 1892, pp. 68–73. |
[12] | Thambugu, D., Duguid, S., Loewen, L., Rolwand, G., Booker, H., You F, M., Cloutier., S. (2013) Genetic variation of six desaturase genes in flax and their impact on fatty acids composition, Theor, Genet 126 (10): 2627–2641. doi: 10.1007/s00122-013-2161-2. |
[13] | Yan, L., Chouw, N., Jayaraman, K. (2013) Flax fibre and its composites - A review. Article in Composites Part B Engineering, Vol-ume 56, Pages 296-317. |
[14] | Hatica, H., Yılmaz, H., Gülçin, I. (2018) Antioxidant Activity of Flaxseed (Linum usitatissimum L.) shell and Analysis of Its Poly-phenol Contents by LC-MS/MS. Rec. Nat. Prod. 12: 4 397-402. |
[15] | Potthast, A., Henniges, U. (2008) Phytate treatment of metallo-gallate inks: Investigation of its effectiveness on model and historic paper samples. Article in Restaurator 29: 219–234. |
[16] | Röhrling, J., Potthast, A., Rosenau, T., Lange, T., Borgards, A., Sixta, H., Kosma, P. (2002) A novel method for the determination of carbonyl groups in cellulosics by fl uorescence labeling. 2. Validation and applications. Biomacromolecules 3: 969–975. |
[17] | Streble, M. (2012) Potassium Permanganate Bleaching of an 18th Century Hand Coloured Aquatint Printr, Restaurator. Vol. 33, p. 409–428. |
[18] | Vinther, B. (2005) Improving Aging Properties of Paper with Iron-Gall Ink by Interleaving with Papers Impregnated with alkaline buffer and antioxidants, Article in Restaurator. |
[19] | Hey, M. (1979) The washing and aqueous deacidification of Paper. Pap Conserv 4: 66–79. |
[20] | Afsharpour, M., Imani, S. (2016) Preventive protection of paper works by using nanocomposite coating of Zinc oxide. Elsevier, http://dx.doi.org/10.1016/j.culher.2016.12.007. |
[21] | Junior, J. (1999) The development of Micro-analytical methodologies for the characterization of the condition of paper, 9th International Congress of IADA. Copenhagen, August 15-21, 107-114. |
[22] | Abdel-Maksoud, G. (2011) Analytical techniques used for the evaluation of a 19th century quranic manuscript conditions, Elsevier, Measurement 44, pp. 1606–1617. |
[23] | George, W. (1995) Hand Book of Material Weathering. second ed., Chem Tec, Ontario, Canada. |
[24] | Neevel, G., Reißland, B. (2005) Bathophenanthroline Indicator Paper Development of a New Test for Iron Ions. Papier Restaurier-ung Vol. 6, No. 1. P 49. |
[25] | Anwar, W., Mohamed, A., Rabee, R., Kamel, A. (2018) A new approach to the treatment of Iron gall ink corrosion using plant Biomass, Mediterranean Archaeology and Archaeometry. Vol. 18, No 2, pp. 35-47. |
[26] | M, Strlic., J, Kolar., D. Kocar., T, Drnovsek., V. S, Selih., R, Susic., B, Pihlar. (2004) What is the pH of alkaline paper?, Journal of e-Preservation Science, pp 35–47. |
[27] | Birstein, V. J., and Tul'chinsky, V. M. (1981) IR‐spectroscopic analysis of aged gelatins, in ICOM committee for conservation, 6th Triennial Meeting, Ottawa, September 21–25, preprints, 1– 8, ICOM, Paris. |
[28] | CALVINI, P., GORASSINI, A. (2002) FTIR–Deconvolution Spectra of Paper Documents., Restaurator 23 (1): 48-66. |
[29] | Abdel-Maksoud, G., El-Amin, A. (2013) The investigation and conservation of a gazelle mummy from the late period in ancient Egypt, Mediterranean Archaeology and Archaeometry, Vol. 13, No 1, pp. 45-67. |
[30] | Rushdya Rabee Ali Hassan. (2015) behavior of archaeological paper after cleaning byorganic solvents under heat accelerated aging, Mediterranean Archaeology andArchaeometry, Vol. 15, No 3, pp. 141-150, DOI: 10.5281/zenodo.18365. |
APA Style
Wafika Noshyutta, Rushdya Rabee Ali Hassan, Mohamed Awd. (2020). Treatment of Paper Oxidation and Acidification by Linseed Gel with MgHCO3 and Zinc Oxide (NP). International Journal of Archaeology, 8(1), 6-14. https://doi.org/10.11648/j.ija.20200801.12
ACS Style
Wafika Noshyutta; Rushdya Rabee Ali Hassan; Mohamed Awd. Treatment of Paper Oxidation and Acidification by Linseed Gel with MgHCO3 and Zinc Oxide (NP). Int. J. Archaeol. 2020, 8(1), 6-14. doi: 10.11648/j.ija.20200801.12
AMA Style
Wafika Noshyutta, Rushdya Rabee Ali Hassan, Mohamed Awd. Treatment of Paper Oxidation and Acidification by Linseed Gel with MgHCO3 and Zinc Oxide (NP). Int J Archaeol. 2020;8(1):6-14. doi: 10.11648/j.ija.20200801.12
@article{10.11648/j.ija.20200801.12, author = {Wafika Noshyutta and Rushdya Rabee Ali Hassan and Mohamed Awd}, title = {Treatment of Paper Oxidation and Acidification by Linseed Gel with MgHCO3 and Zinc Oxide (NP)}, journal = {International Journal of Archaeology}, volume = {8}, number = {1}, pages = {6-14}, doi = {10.11648/j.ija.20200801.12}, url = {https://doi.org/10.11648/j.ija.20200801.12}, eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ija.20200801.12}, abstract = {Collection paper in museums and libraries and stores suffer from acid hydrolysis and oxidations, many factors catalysis the deterioration by acid hydrolysis and oxidations, such as humidity and temperature and light and fungi, paper contains iron ink and colors based on ions heavy metals such as copper and zinc, air pollution, visible and industry light, Residues of manufacturing processes such as bleaching material, additives such as sizing materials, The study proposes a new antioxidants agent by using Line seed gel with magnesium bicarbonate loaded with Zinc oxide (NP), the positive impact of this treatment was evaluated on thermally accelerated ageing on cotton, linen and wooden samples, the samples was verified by FTIR, tensile strength and elongation measurement, Measurement of color change, PH measurement, aromatic hydroxylation assay, (SEM) scanning Electron microscope, Linseed gel with MgHCO3 and Zinc oxide (NP) results to stabilize inks and stop oxidation that occurred and treatment of free radicals, the inks were most stable, The mechanical properties of the samples have been greatly improved, Linseed gel with magnesium bicarbonate loaded with Zinc oxide (NP) consolidation and treatment the samples, the zinc oxide (NP) nano oxide was observed between the fibers which works to protect the cellulose fibers From degradation.}, year = {2020} }
TY - JOUR T1 - Treatment of Paper Oxidation and Acidification by Linseed Gel with MgHCO3 and Zinc Oxide (NP) AU - Wafika Noshyutta AU - Rushdya Rabee Ali Hassan AU - Mohamed Awd Y1 - 2020/06/08 PY - 2020 N1 - https://doi.org/10.11648/j.ija.20200801.12 DO - 10.11648/j.ija.20200801.12 T2 - International Journal of Archaeology JF - International Journal of Archaeology JO - International Journal of Archaeology SP - 6 EP - 14 PB - Science Publishing Group SN - 2330-7595 UR - https://doi.org/10.11648/j.ija.20200801.12 AB - Collection paper in museums and libraries and stores suffer from acid hydrolysis and oxidations, many factors catalysis the deterioration by acid hydrolysis and oxidations, such as humidity and temperature and light and fungi, paper contains iron ink and colors based on ions heavy metals such as copper and zinc, air pollution, visible and industry light, Residues of manufacturing processes such as bleaching material, additives such as sizing materials, The study proposes a new antioxidants agent by using Line seed gel with magnesium bicarbonate loaded with Zinc oxide (NP), the positive impact of this treatment was evaluated on thermally accelerated ageing on cotton, linen and wooden samples, the samples was verified by FTIR, tensile strength and elongation measurement, Measurement of color change, PH measurement, aromatic hydroxylation assay, (SEM) scanning Electron microscope, Linseed gel with MgHCO3 and Zinc oxide (NP) results to stabilize inks and stop oxidation that occurred and treatment of free radicals, the inks were most stable, The mechanical properties of the samples have been greatly improved, Linseed gel with magnesium bicarbonate loaded with Zinc oxide (NP) consolidation and treatment the samples, the zinc oxide (NP) nano oxide was observed between the fibers which works to protect the cellulose fibers From degradation. VL - 8 IS - 1 ER -